تفاعل #329692

معادلة التفاعل

1,4-naphthalenedicarboxylic acid

2-undecylimidazole

→

1,4-naphthalenedicarboxylic acid 2-undecylimidazole

المذيبات

ethyl acetate

ظروف التفاعل

المعالجة

1. 1
   درجة الحرارةheated
2. 2
   درجة الحرارةat reflux for 3 hours
3. 3
   درجة الحرارةAfter cooling
4. 4
   ترشيحfiltration and vacuum
5. 5
   أخرىdrying

الإجراء التجريبي

To a 3 L-three neck flask, 43.2 g of 1,4-naphthalenedicarboxylic acid and 44.5 g of 2-undecylimidazole, and 1000 ml of ethyl acetate were added, stirred and heated at reflux for 3 hours. After cooling, by performing filtration and vacuum drying, 85.9 of the clathrate complex of 1,4-naphthalenedicarboxylic acid/2-undecylimidazole (1:1) was obtained. The obtained clathrate complex was subjected to 1H-NMR, TG-DTA and XRD to confirm the clathration.

المصدر