تفاعل #322192

ord-101062a907d3460c9d4de32380196238

معادلة التفاعل

Nc1nc(N)c(-c2cc(Cl)cc(Cl)c2Cl)c(C(F)(F)F)n1
compound
Nc1nc(N)c(-c2cc(Cl)cc(Cl)c2Cl)c(C(F)(F)F)n1
2,4-Diamino-5-(2,3,5-trichlorophenyl)-6-trifluoromethyl pyrimidine
N#CCc1ccc(Cl)c(Cl)c1
3,4-dichlorophenylacetonitrile
Nc1nc(N)c(-c2ccc(Cl)c(Cl)c2)c(C(F)(F)F)n1
2,4-Diamino-5-(3,4-dichlorophenyl)-6-trifluoromethyl-pyrimidine

المذيبات

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

الإجراء التجريبي

This compound was made in an analogous manner to the compound of Example 4, from 3,4-dichlorophenylacetonitrile (Aldrich) mp. 252°-254.5° C.: TLC (SiO2 ; methanol/chloroform, 1:9) Rf=0.38.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US05597828uspto-grants-1997_01