تفاعل #314910

معادلة التفاعل

(3-Fluoro-phenyl)-(5-nitro-1H-indazol-3-yl)-amine

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title compound

N3-(3-Fluoro-phenyl)-1H-indazole-3,5-diamine

المذيبات

methanol

ظروف التفاعل

المعالجة

1. 1
   أخرىto be consumed
2. 2
   تركيزThe filtrate was concentrated

الإجراء التجريبي

To a solution of (3-Fluoro-phenyl)-(5-nitro-1H-indazol-3-yl)-amine (0.36 g, 1.3 mmol) in methanol (10 ml) was added 10% Pd/C (72 mg). The mixture was allowed to stir at room temperature under H2 atmosphere. After TLC showed the starting material to be consumed, the reaction was passed through a plug of celite. The filtrate was concentrated to give the title compound as an off-white solid. MS (ESI) m/z=243 [M+H]+.

المصدر