تفاعل #312586

معادلة التفاعل

thioanisole

dimethyl sulfate

water

→

dimethylphenylsulfonium sulfate

المذيبات

diethyl ether

ظروف التفاعل

المعالجة

1. 1
   أخرىseparated into two layers

الإجراء التجريبي

6.2 g (0.05 mole) of thioanisole and 6.9 g (0.055 mole) of dimethyl sulfate were stirred for 12 hours at room temperature. 100 g of water and 50 ml of diethyl ether were added to the reaction solution whereupon the mixture separated into two layers. The aqueous layer was taken out, which was an aqueous solution of the target compound, dimethylphenylsulfonium sulfate.

المصدر