تفاعل #312585

معادلة التفاعل

phenacyl bromide

tetrahydrothiophene

water

diethyl ether

→

phenacyltetrahydrothiophenium bromide

المذيبات

nitromethane

ظروف التفاعل

المعالجة

1. 1
   أخرىseparated into two layers

الإجراء التجريبي

88.2 g (0.44 mole) of phenacyl bromide and 39.1 g (0.44 mole) of tetrahydrothiophene were dissolved in 220 g of nitromethane, which was stirred for 4 hours at room temperature. 800 g of water and 400 g of diethyl ether were added to the reaction solution whereupon the mixture separated into two layers. The aqueous layer was taken out, which was an aqueous solution of the target compound, phenacyltetrahydrothiophenium bromide.

المصدر