تفاعل #312217

ord-e1198668898942678d4e637c61b483ee

معادلة التفاعل

CCCCCCCCCCCCCCCC(=O)O
palmitic acid
[Mg+2].[O-2]
magnesium oxide
CCCCCCCCCCCCCCCC(=O)[O-].CCCCCCCCCCCCCCCC(=O)[O-].[Mg+2]
Magnesium palmitate

المتفاعلات

الكواشف

لا شيء

المذيبات

ظروف التفاعل

درجة الحرارة
70°CELSIUS
الظروف التفصيلية
See reaction.notes.procedure_details.

المعالجة

  1. 1
    أخرىAN 223, titer 60° C., particle size >
  2. 2
    أخرىThe hollow-sphered granulate formed
  3. 3
    ترشيحis filtered
  4. 4
    أخرىdried
  5. 5
    workup.WAITThe free fatty acid content amounts to 1.3% but if agitation is carried out for 60 minutes

الإجراء التجريبي

25 g of powdered palmitic acid (AN 223, titer 60° C., particle size >40μ) and 2.1 g of 96% active magnesium oxide (precipitated, density 70 g/liter, IN 62) are suspended in 500 ml of water at room temperature. This is followed with stirring for 30 minutes at 55° C. and 2 hours at 70° C. The hollow-sphered granulate formed is filtered and dried. The free fatty acid content amounts to 1.3% but if agitation is carried out for 60 minutes only, the granulate still contains 3% of free fatty acid.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US04235794uspto-grants-1980_11