تفاعل #312217
ord-e1198668898942678d4e637c61b483ee
معادلة التفاعل
palmitic acid
magnesium oxide
→
Magnesium palmitate
المتفاعلات
الكواشف
لا شيء
المذيبات
ظروف التفاعل
درجة الحرارة
70°CELSIUS
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1أخرىAN 223, titer 60° C., particle size >
- 2أخرىThe hollow-sphered granulate formed
- 3ترشيحis filtered
- 4أخرىdried
- 5workup.WAITThe free fatty acid content amounts to 1.3% but if agitation is carried out for 60 minutes
الإجراء التجريبي
25 g of powdered palmitic acid (AN 223, titer 60° C., particle size >40μ) and 2.1 g of 96% active magnesium oxide (precipitated, density 70 g/liter, IN 62) are suspended in 500 ml of water at room temperature. This is followed with stirring for 30 minutes at 55° C. and 2 hours at 70° C. The hollow-sphered granulate formed is filtered and dried. The free fatty acid content amounts to 1.3% but if agitation is carried out for 60 minutes only, the granulate still contains 3% of free fatty acid.