تفاعل #311945

ord-a8b5c3de89444517adf150eafbb00e2e

معادلة التفاعل

C=C(C)C(=O)OC
methylmethacrylate
C=CC(=O)OCCN(CC)CC
2-(N',N'-diethylamino)ethylacrylate
CC(C)(C#N)N=NC(C)(C)C#N
AIBN
C=C(C)C(=O)OCCCCCCCCCCCCCCCCCC
stearylmethacrylate
C=C(C)C(=O)OCCN(CC)CC
2-(N',N'-diethylamino)ethylmethacrylate
C=C(C)C(=O)OC
methylmethacrylate

المذيبات

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

المعالجة

  1. 1
    workup.WAITbeen gassed with nitrogen gas for half an hour

الإجراء التجريبي

A copolymer of 2-(N',N'-diethylamino)ethylmethacrylate, stearylmetacrylate, and methylmethacrylate was prepared by charging 0.048 mole of 2-(N',N'-diethylamino)ethylacrylate, 0.002 moles of stearylmethacrylate and 0.15 moles of methylmethacrylate in a retort containing 0.002 moles of AIBN. The retort had in accordance with Example 1 been gassed with nitrogen gas for half an hour before charging. The components were dissolved in dry benzene.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US04234565uspto-grants-1980_11