تفاعل #3001

معادلة التفاعل

(Z)-3-(3-nitro-4-chlorophenyl)-2-(3,4,5-trimethoxyphenyl)-prop-2-ene-nitrile

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intended compound

المردود 26.7%

(E)-3-(3-nitro-4-chlorophenyl)-2-(3,4,5-trimethoxyphenyl)-prop-2-ene-nitrile

المردود 26.7%

المذيبات

acetone

ظروف التفاعل

المعالجة

1. 1
   أخرىthe solution was reacted in a photochemical apparatus (visible light) for 1 hour
2. 2
   تركيزThe reaction mixture was concentrated
3. 3
   أخرىa half of it was purified on a silica gel plate

الإجراء التجريبي

1.5 g of (Z)-3-(3-nitro-4-chlorophenyl)-2-(3,4,5-trimethoxyphenyl)-prop-2-ene-nitrile was dissolved in 500 ml of acetone and the solution was reacted in a photochemical apparatus (visible light) for 1 hour. The reaction mixture was concentrated and a half of it was purified on a silica gel plate to give 400 mg of the intended compound.

المصدر