تفاعل #2937

معادلة التفاعل

ethyl acetoacetate

diethylamine

→

title compound

المردود 65.7%

N,N Diethyl-3-oxobutyramide

المردود 65.7%

ظروف التفاعل

المعالجة

1. 1
   workup.DISTILLATIONThe crude mixture was distilled at 115°-120° C./9 mmHg

الإجراء التجريبي

40 g (0.31 mol) of ethyl acetoacetate and 24 g (0.33 mol) of diethylamine were stirred in a Parr apparatus at 150° C. for 10'. The crude mixture was distilled at 115°-120° C./9 mmHg, to give 32 g of the title compound.

المصدر