تفاعل #2687

معادلة التفاعل

HCl

n-nonadecyl-n-tetradecyl-n-decylcarbinol

calcium chloride

→

n-nonadecyl-n-tetradecyl-n-decylmethylchloride

المذيبات

methylene chloride

ظروف التفاعل

المعالجة

1. 1
   غسيلThe product mixture is then washed with 1 liter of a 10% sodium carbonate solution
2. 2
   تجفيفThe organic layer is dried with magnesium sulfate
3. 3
   أخرىthe methylene chloride is evaporated off

الإجراء التجريبي

One mole of n-nonadecyl-n-tetradecyl-n-decylcarbinol is added to 0.2 liters of methylene chloride and 0.32 moles calcium chloride. Approximately 1.5 moles of HCl gas is slowly bubbled through the solution. The product mixture is then washed with 1 liter of a 10% sodium carbonate solution. The organic layer is dried with magnesium sulfate and the methylene chloride is evaporated off to give n-nonadecyl-n-tetradecyl-n-decylmethylchloride.

المصدر