تفاعل #2685

معادلة التفاعل

HCl

di-n-decyl-n-tetradecylcarbinol

calcium chloride

→

di-n-decyl-n-tetradecyl-methylchloride

المذيبات

methylene chloride

ظروف التفاعل

المعالجة

1. 1
   غسيلThe product mixture is then washed with 1 liter of a 10% sodium carbonate solution
2. 2
   تجفيفThe organic layer is dried with magnesium sulfate
3. 3
   أخرىthe methylene chloride is evaporated off

الإجراء التجريبي

One mole of di-n-decyl-n-tetradecylcarbinol is added to 0.2 liters of methylene chloride and 0.32 moles calcium chloride. Approximately 1.5 moles of HCl gas is slowly bubbled through the solution. The product mixture is then washed with 1 liter of a 10% sodium carbonate solution. The organic layer is dried with magnesium sulfate and the methylene chloride is evaporated off to give di-n-decyl-n-tetradecyl-methylchloride.

المصدر