تفاعل #2676

معادلة التفاعل

alcohol

2,3-dichloro-4,5bis-[(2-methoxyethoxy)-methoxy]-styrol

m-chloro perbenzoic acid

→

expected product

المردود 99.6%

2,3-dichloro-4,5bis-[(2-methoxyethoxy)-methoxy]-(1,2-epoxy) styrol

المردود 99.6%

المذيبات

AcOEt cyclohexane

cyclo-hexane ethyl acetate

ظروف التفاعل

المعالجة

1. 1
   أخرىwere reacted

الإجراء التجريبي

Using the procedure of Stage D of Example 40, 13.2 g of thee allylic alcohol of Step C and 10.3 g of m-chloro perbenzoic acid were reacted to obtain 13.7 g of the expected product with a Rf=0.25 (AcOEt-cyclohexane 6-4).

المصدر