تفاعل #2542
ord-b04fe9c2f1da4526a30f3f2067ac49b1
معادلة التفاعل
3,4-methylenedioxyaniline
4-nitrobenzoyl chloride
→
title compound
المردود 87.2%
4-Nitro-N-(3,4-methylenedioxyphenyl)benzamide
المردود 87.2%
الكواشف
لا شيء
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
الإجراء التجريبي
Using 3,4-methylenedioxyaniline (1.44 g, 10.5 mmol) and 4-nitrobenzoyl chloride (1.86 g, 10.0 mmol), the procedure of Reference Example 11 was repeated to obtain 2.49 g (87.2%) of the title compound in the form of yellow crystals.