تفاعل #2507809

معادلة التفاعل

pentacene

maleimide

→

pentacene maleimide

المذيبات

dichlorobenzene

ظروف التفاعل

المعالجة

1. 1
   درجة الحرارةThe mixture is cooled to room temperature
2. 2
   ترشيحthe precipitate is filtered
3. 3
   غسيلwashed with toluene
4. 4
   أخرىdried
5. 5
   أخرىRecrystallization from dichlorobenzene

الإجراء التجريبي

A suspension of pentacene (287 mg, 1 mmole) and maleimide (1 mmole) in 4 mL of dichlorobenzene is heated to 160° C. for 4 hours. The mixture is cooled to room temperature and the precipitate is filtered, washed with toluene and dried. Recrystallization from dichlorobenzene affords pure samples of pentacene-maleimide adduct as white needles.

المصدر