تفاعل #2389089

معادلة التفاعل

dodecane thiol

sulfuryl chloride

→

dodecansulfenyl chloride

المذيبات

CHCl3

ظروف التفاعل

المعالجة

1. 1
   أخرىRemoval of solvent (aspirator)

الإجراء التجريبي

To a solution of dodecane thiol (1.00 mL, 4.17 mmol, Aldrich Chemical Company) in 20 mL CHCl3 was added sulfuryl chloride (0.74 mL, 9.18 mmol, Aldrich Chemical Company), and the resulting mixture was stirred at room temperature for 18 h. Removal of solvent (aspirator), afforded dodecansulfenyl chloride that was determined to be sufficiently pure by 1H NMR.

المصدر