تفاعل #2383764
ord-dfd5ee8d4f8142afabf7ec74d7a7bb2d
معادلة التفاعل
4-chloro-3-methylpyrazole
formalin
→
solid
المردود 95.0%
N-hydroxymethyl-4-chloro-3-methylpyrazole
المردود 95.0%
المتفاعلات
الكواشف
لا شيء
المذيبات
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1أخرىWater and methanol were then evaporated
الإجراء التجريبي
116 g (1.0 mol) of 4-chloro-3-methylpyrazole in 50 ml of methanol were dissolved in 100 g (1.0 mol) of formalin solution (30%) at room temperature. Water and methanol were then evaporated. The title compound remained as a white solid (yield 95%).