تفاعل #231

معادلة التفاعل

Ic1ccccc1

CN(C)CCN

→

CN(C)CCNc1ccccc1

المذيبات

CN(C)C=O

ظروف التفاعل

الإجراء التجريبي

In a 50 mL round-bottomed flask (t=g) was unsym-Dimethylethylenediamine (1.080 mL, 9.80 mmol), Iodobenzene (0.549 mL, 4.90 mmol), and TRIS(DIBENZYLIDENEACETONE)DIPALLADIUM(0) (0.449 g, 0.49 mmol)Cesium carbonate (2.396 g, 7.35 mmol) andCesium carbonate (2.396 g, 7.35 mmol) were added. in DMF (10 mL) ([VOLUME]) to give a brown suspension. Reaction stirred over night at 100°C. no reaction.

المصدر