تفاعل #2300068

معادلة التفاعل

Epichlorohydrin

isoeugenol

NaOH

→

4-epoxy isoeugenol

المذيبات

ethanol

ظروف التفاعل

المعالجة

1. 1
   درجة الحرارةto reflux for 2–6 hours
2. 2
   أخرىEthanol was then removed from the resulting mixture
3. 3
   غسيلeluted with n-hexane and ethyl acetate
4. 4
   أخرىdried with reduced pressure

الإجراء التجريبي

To manufacture this combination Epichlorohydrin was mixed with isoeugenol and NaOH dissolved in ethanol and boiled to reflux for 2–6 hours. Ethanol was then removed from the resulting mixture and the mixture was passed through silica gel column eluted with n-hexane and ethyl acetate, and dried with reduced pressure, to obtain 4-epoxy isoeugenol.

المصدر