تفاعل #2275688
ord-3f67295fdaca46fca78f9eca296a8f09
معادلة التفاعل
Acetic acid 3-acetoxy-2-tert-butoxycarbonylamino-propyl ester
trifluoroacetic acid
→
product
2-Acetoxy-1-acetoxymethyl-ethyl-ammonium trifluoroacetate
الكواشف
لا شيء
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1أخرىwhen the volatiles were removed at reduced pressure
الإجراء التجريبي
Acetic acid 3-acetoxy-2-tert-butoxycarbonylamino-propyl ester (7.2 g) was dissolved in trifluoroacetic acid (40 ml) and stirred at ambient temperature. Effervescence was rapid at the start and had stopped after 1 h when the volatiles were removed at reduced pressure to give the product as a viscous oil in quantitative yield.