تفاعل #2267055
ord-1a1a3434cae245c49c2a39443e27ee10
معادلة التفاعل
pentafluorobenzenesulfonyl chloride
tetramethylammonium hydroxide
→
tetramethylammonium pentafluorobenzenesulfonate
الكواشف
لا شيء
المذيبات
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1درجة الحرارةcooling
الإجراء التجريبي
25 gof pentafluorobenzenesulfonyl chloride was dissolved in 100 ml of methanol under ice-cooling. Then 100 g of a 25% aqueous solution of tetramethylammonium hydroxide was slowly added thereto. By stirring at room temperature for 3 hours, a solution of tetramethylammonium pentafluorobenzenesulfonate was obtained. Thus solution was employed in salt exchange between sulfonium salt and iodonium salt.