تفاعل #2267054

ord-641d855038954af3b7002d2a416610d7

معادلة التفاعل

Cc1ccc(S(=O)(=O)O)cc1.O
p-toluenesulphonic acid monohydrate
Oc1cccc(O)c1
resorcinol
Cc1ccc(S(=O)(=O)O)cc1
p-Toluenesulphonic Acid

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

المعالجة

  1. 1
    أخرىAn antireflective composition was prepared
  2. 2
    workup.DISSOLUTIONAfter dissolution
  3. 3
    ترشيحthe solution was filtered through a polypropylene
  4. 4
    ترشيحfilter with a 0.2 um pore size

الإجراء التجريبي

An antireflective composition was prepared by dissolving together 0.6682 g of the polymer of Example 1, 0.1177 g of the trimeric condensate of resorcinol and diethylol-p-cresol (plasticizer), 0.0990 g of Powderlink 1174 crosslinker (from Cytec Industries), an acid crosslinking catalyst consisting of 0.009 g of p-toluenesulphonic acid monohydrate (Aldrich), 0.0072 g of FC 430 surfactant (3M Corp.) and 30.96 g of proylene glycol methyl ether alcohol solvent. After dissolution, the solution was filtered through a polypropylene filter with a 0.2 um pore size.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US06887648B2uspto-grants-2005_05