تفاعل #2204033

معادلة التفاعل

bis(dimethylamino)dichloromethane

p-toluenesulfonic acid monohydrate

→

bis(dimethylamino)chlorocarbenium tosylate

المردود 97.8%

ظروف التفاعل

المعالجة

1. 1
   درجة الحرارةCooling to room temperature

الإجراء التجريبي

3.0 g (17.5 mmol) of bis(dimethylamino)dichloromethane and 3.33 g (17.5 mmol) of p-toluenesulfonic acid monohydrate are mixed. The mixture is heated to 100° C. over the course of 30 min, and a vacuum of 7 Pa is subsequently applied over one hour. Cooling to room temperature gives 5.25 g of bis(dimethylamino)chlorocarbenium tosylate, corresponding to a yield of 97.8%.

المصدر