تفاعل #219897

معادلة التفاعل

3,5-heptandione

2,6-dimethyl-3,5-heptandione

→

2,6-dimethyl-3,5-heptandiol

المردود 90.0%

ظروف التفاعل

المعالجة

1. 1
   أخرىSynthesis procedure
2. 2
   أخرىfinally the product was purified
3. 3
   workup.DISTILLATIONby distilling under reduced pressure

الإجراء التجريبي

Synthesis procedure was similar to that described in synthetic example 19(1), except that 3,5-heptandione was replaced by 2,6-dimethyl-3,5-heptandione, and finally the product was purified by distilling under reduced pressure. 2,6-dimethyl-3,5-heptandiol as a colorless liquid was obtained with a yield of 90%.

المصدر