تفاعل #216076

معادلة التفاعل

Octadecylamine

Glycidol

→

white solid

المردود 95.9%

3-Octadecylamino-1,2-Dihydroxy-Propane

المردود 95.9%

المذيبات

methanol

ظروف التفاعل

المعالجة

1. 1
   درجة الحرارةunder reflux for one additional hour
2. 2
   درجة الحرارةcooled to room temperature
3. 3
   أخرىevaporated to dryness

الإجراء التجريبي

Octadecylamine (18 g) was dissolved in 200 ml methanol and heated to 60° C. Glycidol (4.95 g) was added dropwise under constant stirring over one and half hours. The reaction mixture was kept under reflux for one additional hour, and then cooled to room temperature, and evaporated to dryness, resulting in 22 g white solid material. This was then recrystallized from hexane, to yield ODP, mp 81°-83° C.

المصدر