تفاعل #2160379

معادلة التفاعل

3H,6H-1,4,5a,8a-tetraazaacenaphthylen-3-one

5-(Methylthio)-8-[3-(trifluoromethyl)phenyl]-3H,6H-1,4,5a,8a-tetraazaacenaphthylen-3-one

→

product

5-[(Phenylmethyl)amino)-8-[3-(trifluoromethyl)phenyl]-3H,6H-1,4,5a,8a-tetraazaacenaphthylen-3-one

المذيبات

benzylamine

ظروف التفاعل

المعالجة

1. 1
   ترشيحfiltered
2. 2
   غسيلThe solid on the filter was washed with ether and air
3. 3
   أخرىdried

الإجراء التجريبي

A 200 mg amount of 5-(methylthio)-8-[3-trifluoromethyl)phenyl]-3H,6H-1,4,5a,8a-tetraazaacenaphthylen-3-one (prepared as described in Example 9) was suspended in 10.0 ml of benzylamine. The reaction mixture was cooled to room temperature and filtered. The solid on the filter was washed with ether and air dried to give 189 mg of the product of the example as a white solid, m.p. 220°-224° C.

المصدر