تفاعل #2148490

ord-0c8dfe4cea5c4620a20654170e9a657a

معادلة التفاعل

CC(C)(C)c1ccc(S(=O)c2ccc(C(C)(C)C)cc2)cc1
bis (4-tert-butylphenyl)sulfoxide
CC(C)(C)c1ccc(Br)cc1
4-tert-butyl bromobenzene
CC(C)(C)c1ccc([S+](c2ccc(C(C)(C)C)cc2)c2ccc(C(C)(C)C)cc2)cc1.[Br-]
Tris(4-tert-butylphenyl)Sulfonium Bromide

الكواشف

لا شيء

المذيبات

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

المعالجة

  1. 1
    أخرىThe intended compound was obtained in a similar manner to that

الإجراء التجريبي

The intended compound was obtained in a similar manner to that of Synthesis Example 1-1 except that bis (4-tert-butylphenyl)sulfoxide was used instead of diphenylsulfoxide, 4-tert-butyl bromobenzene was used instead of chlorobenzene, and the amount of water was increased at the time of extraction.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US08283104B2uspto-grants-2012_10