تفاعل #214314

معادلة التفاعل

2-Bromomethyl-4,5-dimethyl-1,3-dioxolane

methylamine

→

N-(4,5-dimethyl-1,3-dioxolan-2-ylmethyl)methylamine

ظروف التفاعل

المعالجة

1. 1
   أخرىfitted with a mechanical stirrer
2. 2
   استخلاصThe reaction mixture was then extracted with diethyl ether
3. 3
   أخرىThe extract was dried
4. 4
   أخرىa rotary evaporator

الإجراء التجريبي

2-Bromomethyl-4,5-dimethyl-1,3-dioxolane (100 grams) and 40% aqueous methylamine (300 ml) were charged into a glass reaction vessel fitted with a mechanical stirrer and thermometer and were stirred at room temperature for a period of about 14 hours. The reaction mixture was then extracted with diethyl ether. The extract was dried and the ether stripped off using a rotary evaporator to yield the desired product N-(4,5-dimethyl-1,3-dioxolan-2-ylmethyl)methylamine as the residue.

المصدر