تفاعل #2139926

ord-30ba1818977d4670a24a24a0170e33ea

معادلة التفاعل

C=COCC
Ethyl vinyl ether
OCc1ccccc1
benzyl alcohol
C=COCc1ccccc1
benzyl vinyl ether

الكواشف

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

المعالجة

  1. 1
    استخلاصThe reaction mixture was extracted with ethyl acetate
  2. 2
    استخلاصthe ethyl acetate extract
  3. 3
    غسيلwas washed with water
  4. 4
    workup.DISTILLATIONfollowed by distillation in vacuo

الإجراء التجريبي

Ethyl vinyl ether was mixed in benzyl alcohol, to which was then added mercury acetate, and the mixture was stirred at room temperature for 12 hours. The reaction mixture was extracted with ethyl acetate and the ethyl acetate extract was washed with water, followed by distillation in vacuo to obtain benzyl vinyl ether.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US07326513B2uspto-grants-2008_02