تفاعل #2069924

معادلة التفاعل

Acetic anhydride

4-isopropylaniline

→

N-Acetyl-4-isopropylaniline

المذيبات

chloroform

ظروف التفاعل

المعالجة

1. 1
   درجة الحرارةIn the course of this, intense heating of the reaction mixture
2. 2
   workup.ADDITIONOn completion of the dropwise addition
3. 3
   تركيزThe reaction mixture is concentrated to dryness
4. 4
   أخرىthe resulting, reddish-white solid is recrystallized from hexane

الإجراء التجريبي

Acetic anhydride (26.0 g, 254 mmol) is slowly added dropwise to a solution of 4-isopropylaniline (17.2 g, 127 mmol) in 80 ml of chloroform. In the course of this, intense heating of the reaction mixture occurs. On completion of the dropwise addition, the mixture is stirred at room temperature for another 2 h. The reaction mixture is concentrated to dryness and the resulting, reddish-white solid is recrystallized from hexane.

المصدر