تفاعل #2021839

معادلة التفاعل

2-fluoro-5-nitro-N-(1,3-benzodioxol-5-ylmethyl)benzamide

2-amino-1-hexanol

→

2-[1-(1-Hydroxymethyl)pentylamino]-5-nitro-N-(1,3-benzodioxol-5-ylmethyl)benzamide

المردود 77.8%

ظروف التفاعل

الإجراء التجريبي

2-[1-(1-Hydroxymethyl)pentylamino]-5-nitro-N-(1,3-benzodioxol-5-ylmethyl)benzamide (203 mg) was prepared from 2-fluoro-5-nitro-N-(1,3-benzodioxol-5-ylmethyl)benzamide (200 mg) and 2-amino-1-hexanol (221 mg) in a similar manner to that of Example 1(1) as yellow crystals. mp 112-115° C.

المصدر