تفاعل #2021473

معادلة التفاعل

perfluorooctanesulfonic acid

silver carbonate

→

silver perfluorooctanesulfonate

المذيبات

water

ظروف التفاعل

المعالجة

1. 1
   workup.ADDITIONwas added
2. 2
   workup.STIRRINGAfter stirring at room temperature for 3 days
3. 3
   ترشيحthe mixture was filtered
4. 4
   ترشيحthe obtained filter-cake
5. 5
   غسيلwas washed with 10 parts of ion-exchange water
6. 6
   تجفيف20 parts of diethylether and dried

الإجراء التجريبي

Into a four-necked flask were charged 75 parts of perfluorooctanesulfonic acid and 100 parts of water, and 21.4 parts of silver carbonate was added thereto with stirring. After stirring at room temperature for 3 days, the mixture was filtered and the obtained filter-cake was washed with 10 parts of ion-exchange water, then 20 parts of diethylether and dried to give 60.3 parts of silver perfluorooctanesulfonate.

المصدر