تفاعل #2008586

معادلة التفاعل

5-(5-Ethyl-2-methyl-6-oxo-1,6-dihydropyridin-3-yl)furan-2-sulfonyl chloride

(2-morpholin-4-yl)ethylamine

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title compound

المردود 51.0%

5-(5-Ethyl-2-methyl-6-oxo-1,6-dihydropyridin-3-yl)furan-2-sulfonic acid (2-morpholin-4-yl)ethylamide hydrochloride

المردود 51.0%

ظروف التفاعل

الإجراء التجريبي

5-(5-Ethyl-2-methyl-6-oxo-1,6-dihydropyridin-3-yl)furan-2-sulfonyl chloride is reacted with (2-morpholin-4-yl)ethylamine as described in Step 5, Example 24 to give the title compound as a solid (51% yield). LC/MS: RT 1.93 min; m/e 396 (M+H); 1H NMR (δ, ppm): 11.85 (1H, s), 8.46 (1H, t), 7.52 (1H, s), 7.24 (1H, d); 6.73 (1H, d), 3.85 (4H, m), 3.12 (8H, m), 2.49 (5H), 1.11 (3H, t).

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