تفاعل #1992997

معادلة التفاعل

5-(2-methoxy-benzylidene)-hydantoin

→

desired compound

المردود 79.0%

5-(2-methoxy-benzyl)-hydantoin

المردود 79.0%

المذيبات

sodium hydroxide

ظروف التفاعل

المعالجة

1. 1
   workup.ADDITIONare added

الإجراء التجريبي

218.2 g (1 mole) of 5-(2-methoxy-benzylidene)-hydantoin are dissolved in 2 l of a N sodium hydroxide solution and 70 g of wet Raney-nickel are added. The reaction mixture is worked up according to Example 6. Thus 174 g of the desired compound are obtained, yield 79%. Mp.: 186° C.

المصدر