تفاعل #1960492
ord-39843891419c41f6acc794de2578ff4d
معادلة التفاعل
7,8-difluoro-2-pentyl-2H-chromene
→
7,8-difluoro-2-pentylchroman
المتفاعلات
الكواشف
المذيبات
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1أخرىThe batch is evaporated to dryness
الإجراء التجريبي
51.0 g (0.21 mol) of 7,8-difluoro-2-pentyl-2H-chromene are hydrogenated at RT for 1 h in 510 ml of toluene in the presence of Pd/C (5% of Pd). The batch is evaporated to dryness: the crude product (yellowish liquid) can be used directly for the next step.