تفاعل #1925213

ord-91cc6f18619344abb0dfe1b2e94b06e2

معادلة التفاعل

C=CC(=O)OC
methyl acrylate
OCCNCCO
diethanolamine
COC(=O)CCN(CCO)CCO
N,N-bis(2-hydroxyethyl)-2-(methoxycarbonyl)ethylamine
المردود 98.0%

المتفاعلات

الكواشف

لا شيء

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

المعالجة

  1. 1
    تركيزThe reaction mixture was concentrated under reduced pressure

الإجراء التجريبي

At 20 to 30° C., 9.01 g of methyl acrylate was added to 10.0 g of diethanolamine. The resulting mixture was allowed to stand for 20 hours. The reaction mixture was concentrated under reduced pressure, whereby N,N-bis(2-hydroxyethyl)-2-(methoxycarbonyl)ethylamine was obtained (yield: 98%).

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US06673511B1uspto-grants-2004_01