تفاعل #1925213
ord-91cc6f18619344abb0dfe1b2e94b06e2
معادلة التفاعل
methyl acrylate
diethanolamine
→
N,N-bis(2-hydroxyethyl)-2-(methoxycarbonyl)ethylamine
المردود 98.0%
المتفاعلات
الكواشف
لا شيء
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1تركيزThe reaction mixture was concentrated under reduced pressure
الإجراء التجريبي
At 20 to 30° C., 9.01 g of methyl acrylate was added to 10.0 g of diethanolamine. The resulting mixture was allowed to stand for 20 hours. The reaction mixture was concentrated under reduced pressure, whereby N,N-bis(2-hydroxyethyl)-2-(methoxycarbonyl)ethylamine was obtained (yield: 98%).