تفاعل #1906699

معادلة التفاعل

1-chlorohexadecane

1-benzyl-2-methyl imidazole

→

1-benzyl-2-methyl-3-hexadecyl imidazolium chloride

ظروف التفاعل

المعالجة

1. 1
   أخرىwas set from 75 to 80° C
2. 2
   workup.WAITThe reaction was continued for four days
3. 3
   غسيلThen, the product was washed with ethyl acetate five times
4. 4
   أخرىAfter that, it was dried under vacuum for three days

الإجراء التجريبي

The procedure of Example 1 was repeated with minor change. 427 g of 1-chlorohexadecane (Aldrich) and 280 g of 1-benzyl-2-methyl imidazole (Shikoku Chemicals Corp. 1B2MZ) were added into a 2000 ml three-neck round-bottom flask. The reaction temperature was set from 75 to 80° C. After four hours the milk-like solution transferred into a homogenous solution. The reaction was continued for four days. Then, the product was washed with ethyl acetate five times. After that, it was dried under vacuum for three days.

المصدر