تفاعل #1876821

ord-a9e2bc7ece64422aa680ac0d6978bd7c

المذيبات

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

المعالجة

  1. 1
    أخرىReaction
  2. 2
    أخرىwas carried out at room temperature

الإجراء التجريبي

The 1,3-dichloroformyl-5-hydroxyadamantane was dissolved in methylene chloride. To this solution were added a small amount of trimethylamine, and then an eguimolar amount of trimethylsilyl chloride. Reaction was carried out at room temperature to obtain 1,3-dichloroformyl-5-trimethylsiloxyadamantane.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US07070905B2uspto-grants-2006_07