تفاعل #1846326

ord-2500a6f6be2348068c0f6a5f8692966b

معادلة التفاعل

C=C(C)C(=O)O
MAA
C=C(C)C(=O)O
methacrylic acid
C=C(C)C(=O)OCCCCCCCCCCCCCCCCCC
SMA
OCCS
2-mercaptoethanol
C=C(C)C(=O)OCCCCCCCCCCCCCCCCCC
stearyl methacrylate
C=C(C)C(=O)O.C=C(C)C(=O)OCCCCCCCCCCCCCCCCCC
Stearyl Methacrylate Methacrylic Acid

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

المعالجة

  1. 1
    أخرىat 25° C.
  2. 2
    أخرىat 25° C.

الإجراء التجريبي

The resultant product contained 24.64 percent by weight of a 1:2 copolymer of stearyl methacrylate (SMA) and methacrylic acid (MAA), 0.61 percent residual SMA; less than 0.02 percent residual MAA; no initiator; less than 0.05 percent 2-mercaptoethanol; and had a bulk viscosity at 25° C. of about 4000-5000 centipoise. When the product was diluted to 10% polymeric solids with further oil, the solution had a viscosity at 25° C. of 36-46 centipoise.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US04339373uspto-grants-1982_07