تفاعل #1827523

معادلة التفاعل

N,N-dimethylhexylamine

1-bromo-3-chloropropane

→

(3-chloropropyl)hexyl-dimethylammonium bromide

المذيبات

methanol

ظروف التفاعل

المعالجة

1. 1
   أخرىA 500 mL, 3-necked, round-bottomed flask equipped with air condensers
2. 2
   أخرىSolvent was removed by rotary evaporation under reduced pressure
3. 3
   أخرىto yield a brown, viscous oil

الإجراء التجريبي

A 500 mL, 3-necked, round-bottomed flask equipped with air condensers and a magnetic stirring plate was charged with N,N-dimethylhexylamine (199.46 grams, 1.54 moles), 1-bromo-3-chloropropane (243.00 grams, 1.54 moles) and 250 mL of methanol. The reaction was maintained at 65° C. for 24 hours. Solvent was removed by rotary evaporation under reduced pressure to yield a brown, viscous oil. Yield 445.8 grams (1.55 moles, 100%).

المصدر