تفاعل #1810810
ord-358755067df943e3b6940451c3eff180
معادلة التفاعل
1-(trans-4-aminocyclohexyl)-1-methyl-thiourea
hydrochloride
methyliodide
→
hydrochloride
hydroiodide
1-(trans-4-aminocyclohexyl)-1,2-dimethyl-isothiourea
الكواشف
لا شيء
المذيبات
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1درجة الحرارةis refluxed for 2 hours
- 2أخرىsolvent is evaporated
الإجراء التجريبي
A mixture of 0.6 g of 1-(trans-4-aminocyclohexyl)-1-methyl-thiourea in the form of a hydrochloride in 30 ml of MeOH and 0.22 ml of methyliodide is refluxed for 2 hours, solvent is evaporated and 1-(trans-4-aminocyclohexyl)-1,2-dimethyl-isothiourea in the form of a hydrochloride and a hydroiodide is obtained.