تفاعل #1782810

معادلة التفاعل

rac-N2-(7-Methoxy-indan-1-yl)-4H-benzo[d][1,3]oxazine-2,6-diamine

rac-N2-(7-methoxy-indan-1-yl)-4H-benzo[d][1,3]oxazine-2,6-diamine

piperidine-1-sulfonyl chloride

→

title compound

المردود 75.0%

rac-Piperidine-1-sulfonic acid [2-(7-methoxy-indan-1-ylamino)-4H-benzo[d][1,3]oxazin-6-yl]-amide

المردود 75.0%

ظروف التفاعل

الإجراء التجريبي

Prepared from rac-N2-(7-methoxy-indan-1-yl)-4H-benzo[d][1,3]oxazine-2,6-diamine (Example 10) (100 mg, 0.323 mmol) and piperidine-1-sulfonyl chloride (65 mg, 0.353 mmol) according to the procedure described for Example 27. Obtained the title compound as a light yellow foam (110 mg, 75%), MS (ISP) m/e=457.4 [(M+H)+].

المصدر