تفاعل #1772058

معادلة التفاعل

trimethoxysilane

acetic acid

10-(methoxymethoxy)-1-decene

→

target compound

المردود 81.4%

10-(methoxymethoxy)decyltrimethoxysilane

المردود 81.4%

المذيبات

tetrahydrofuran

ظروف التفاعل

المعالجة

1. 1
   أخرىat 80° C
2. 2
   workup.DISTILLATIONdistilled under reduced pressure

الإجراء التجريبي

Under a nitrogen atmosphere, 64 g of trimethoxysilane and 0.57 g of acetic acid were dropped in a mixture of 100 g of 10-(methoxymethoxy)-1-decene and a catalytic amount of a solution of platinate chloride in tetrahydrofuran at 80° C. The reaction mixture was stirred at 80° C. for 3 hours, and distilled under reduced pressure to yield 131 g of a target compound.

المصدر