تفاعل #1766453

معادلة التفاعل

3-phenylindole

hydrofluoroboric acid

→

3-phenylindoline

المردود 47.0%

المذيبات

ethanol

ظروف التفاعل

الإجراء التجريبي

A mixture of 4.0 g of 3-phenylindole, 80 ml of 86% ethanol, 35 ml of 48% hydrofluoroboric acid and 0.25 g of 10% Pd/C was hydrogenated at 60 p.s.i. and 60° C for 18 hours. The reaction mixture was worked up as in Example 2 and 1.9 g of pure 3-phenylindoline was obtained.

المصدر