تفاعل #1764048

معادلة التفاعل

diethylmethylamine

p-toluenesulfonic acid monohydrate

→

diethylmethylamine

p-toluenesulfonic acid

المذيبات

2-butanone

ظروف التفاعل

المعالجة

1. 1
   workup.DISTILLATIONthe solvent was then distilled off in vacuo
2. 2
   أخرىThe obtained solid was recrystallized from acetone

الإجراء التجريبي

3.0 g of diethylmethylamine was dissolved in 30 cm3 of 2-butanone, to which was then gradually added 5.7 g of p-toluenesulfonic acid monohydrate while stirring. The stirring was continued for an additional one hour, and the solvent was then distilled off in vacuo. The obtained solid was recrystallized from acetone to obtain a diethylmethylamine salt of p-toluenesulfonic acid.

المصدر