تفاعل #1702112

معادلة التفاعل

2-(3-nitrophenyl)ethanol

→

desired product

المردود 99.0%

2-(3-Aminophenyl)ethanol

المردود 99.0%

المذيبات

methanol

ظروف التفاعل

المعالجة

1. 1
   أخرىwas hydrogenated at 45 psi overnight
2. 2
   ترشيحThe resultant mixture was filtered
3. 3
   تركيزconcentrated

الإجراء التجريبي

Into a pressure bottle were added 2-(3-nitrophenyl)ethanol (3.0 g, 18 mmol) and methanol (100 mL) and 10% palladium on carbon (0.1 g, 0.08 mmol). The reaction mixture was hydrogenated at 45 psi overnight. The resultant mixture was filtered and concentrated to provide the desired product (2.44 g, 99%) as a white solid. LCMS for C8H12NO (M+H)+: m/z=138.1.

المصدر