تفاعل #1687677
ord-e9c2f5d9ccaa46e5b74c358a16261713
معادلة التفاعل
p-tert-butoxystyrene
styrene
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p-tert-butoxystyrene styrene
المتفاعلات
الكواشف
لا شيء
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1أخرىmaterials, polymerization reaction
الإجراء التجريبي
Using 81.1 g (0.46 mol) of p-tert-butoxystyrene and 4.6 g (0.04 mol) of styrene as starting materials, polymerization reaction and after-treatments were carried out according to the procedure of (1) of Preparation Example 1 to give 77.1 g of poly(p-tert-butoxystyrene/styrene) as white powdery crystal. P-tert-butoxystyrene unit/styrene unit molar ratio in the polymer≈92:8 (1H NMR). Mw≈20,000 (GPC with polystyrene calibration).