تفاعل #1687672

ord-8ed2e921bb1241bcb783c5c758d97255

معادلة التفاعل

CC(=O)CC(C)=O
acetylacetone
O.O.O.O.O.O.O=[N+]([O-])[O-].O=[N+]([O-])[O-].O=[N+]([O-])[O-].[Ce+3]
cerium nitrate hexahydrate
→
O=[N+]([O-])[O-].O=[N+]([O-])[O-].O=[N+]([O-])[O-].[Ce+3]
cerium nitrate

المتفاعلات

CC(=O)CC(C)=O
acetylacetone
O.O.O.O.O.O.O=[N+]([O-])[O-].O=[N+]([O-])[O-].O=[N+]([O-])[O-].[Ce+3]
cerium nitrate hexahydrate

الكواشف

لا شيء

ظروف التفاعل

درجة الحرارة
90°CELSIUS
الظروف التفصيلية
See reaction.notes.procedure_details.

المعالجة

  1. 1
    workup.ADDITIONwas treated for 1 hour

الإجراء التجريبي

3 moles of acetylacetone was added to 1 mole of cerium nitrate hexahydrate and heated to 90° C. under agitation under which the mixture was treated for 1 hour. The solution was provided as cerium nitrate stock solution. This had a CeO2 solid content of 23.2%.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US05976678uspto-grants-1999_11