تفاعل #1687647
ord-8eb39357567449b8b708235f99951a97
معادلة التفاعل
( 3 )
4-acetoxy-2-fluoro-1-(1-ethylpropyloxycarbonyl)benzene
benzylamine
→
4-hydroxy-2-fluoro-1-(1-ethylpropyloxycarbonyl)benzene
الكواشف
لا شيء
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1غسيلthe diluted mixture was washed with diluted hydrochloric acid
- 2تجفيفwith water and dried over magnesium sulfate
الإجراء التجريبي
0.5 Gram of the compound obtained in the above (3) was dissolved in 30 ml of ethanol, and 1.5 g of benzylamine was added dropwise thereto. Further, the mixture was stirred at room temperature for one day and diluted with 300 ml of ether, and the diluted mixture was washed with diluted hydrochloric acid and then with water and dried over magnesium sulfate.