تفاعل #1687635
ord-1f3d63b3d76045508493ba53e1f22655
معادلة التفاعل
fumarate
88
5-Methyl-2-(3-pyridyl)-thiazole
→
title compound
5-Methyl-2-(1-methyl-1,2,5,6-tetrahydro-3-pyridyl)-thiazole
الكواشف
لا شيء
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1أخرىThe crude free base obtained
الإجراء التجريبي
The title compound was prepared from 88 (2.2 g, 0.013 mol) by the procedure described in Example 49. The crude free base obtained, 89, was converted to the title fumarate, 90. Yield: 0.8 g (0.0032 mol, 25%). M.P. 159°-160° C. Anal. (C12H16N2O2S)C, H, N.