تفاعل #1635
ord-8ac817860d9d44d4acd7988671266af2
معادلة التفاعل
n-hexylphosphinic acid, n-butyl ester
paraformaldehyde
→
title compound
n-Hexylhydroxymethylphosphinic acid, n-butyl ester
الكواشف
لا شيء
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1أخرىPurification by chromatography
- 2غسيلeluting with dichloromethane containing 5% methanol
- 3أخرىgave an oil
الإجراء التجريبي
The title compound was prepared from n-hexylphosphinic acid, n-butyl ester and paraformaldehyde according to the method described in Procedure 31. Purification by chromatography, eluting with dichloromethane containing 5% methanol, gave an oil.